Pergamon Series in Analytical Chemistry, Volume 2: Basic Analytical Chemistry brings together numerous studies of the vast expansion in the use of classical and instrumental methods of analysis. This book is composed of six chapters. After providing a theoretical background of analytical chemistry, this book goes on dealing with the fundamental principles of chemical equilibria in solution. The subsequent chapters consider the advances in qualitative and quantitative chemical analyses. These chapters present a unified view of these analyses based on the Bronsted-Lowry theory and the donor-acceptor principle. These topics are followed by discussions on instrumental analysis using various methods, including electrochemical, optical, spectroscopic, and thermal methods, as well as radioactive isotopes. The finals chapters examine the separation methods and the essential features of organic chemical analysis that are different from methods for inorganic compounds. This book is of value to analytical chemists and researchers.
BASIC ANALYTICAL CHEMISTRY Malaysia is a fast developing country. Realizing the need to provide experts in chemistry,this book is appropriate to be used as a text for fundamental course in analytical chemistry. The texts cover topics from the most basic analytical chemistry course including methods on basic analyses to important concepts such as handling of data analysis, chemical equilibrium, stoichiometry and titration. The chemical equilibrium in this book covers acid-base equilibrium, precipitation, complex and redox titration. For every topic, examples and solutions are provided to give reader a better understanding in the topics covered.
Analytical Chemistry Has Made Significant Progress In The Last Two Decades. Several Methods Have Come To The Forefront While Some Classical Methods Have Been Relegated. An Attempt Has Been Made In This Edition To Strike A Balance Between These Two Extremes, By Retaining Most Significant Methods And Incorporating Some Novel Techniques. Thus An Endeavour Has Been Made To Make This Book Up To Date With Recent Methods.The First Part Of This Book Covers The Classical Volumetric As Well As Gravimetric Methods Of Analysis. The Separation Methods Are Prerequisite For Dependable Quantitative Methods Of Analysis. Therefore Not Only Solvent Extraction Separations But Also Chromatographic Methods Such As Adsorption, Partition, Ion- Exchange, Exclusion Andelectro Chromatography Have Been Included. To Keep Pace With Modern Developments The Newly Discovered Techniques Such As Ion Chromatography, Super-Critical Fluid Chromatography And Capillary Electrophoresis Have Been Included.The Next Part Of The Book Encompases The Well Known Spectroscopic Methods Such As Uv, Visible, Ir, Nmr, And Esr Techniques And Also Atomic Absorption And Plasma Spectroscopy And Molecular Luminescences Methods. Novel Analytical Techniques Such As Auger, Esca And Photo Accoustic Spectroscopy Of Surfaces Are Also Included.The Final Part Of This Book Covers Thermal And Radioanalytical Methods Of Analysis. The Concluding Chapters On Electroanalytical Techniques Include Potientometry, Conductometry. Coulometry And Voltametry Inclusive Of All Kinds Of A Polarography. The Theme Of On Line Analysis Is Covered In Automated Methods Of Analysis.To Sustain The Interest Of The Reader Each Chapter Is Provided With Latest References To The Monographs In The Field. Further, To Test The Comprehension Of The Subject Each Chapter Is Provided With Large Number Of Solved And Unsolved Problems.This Book Should Be Useful To Those Reads Who Have Requisite Knowledge In Chemistry And Are Majoring In Analytical Chemistry. It Is Also Useful To Practising Chemists Whose Sole Aim Is To Keep Abreast With Modern Developments In The Field.
Enables students to progressively build and apply new skills and knowledge Designed to be completed in one semester, this text enables students to fully grasp and apply the core concepts of analytical chemistry and aqueous chemical equilibria. Moreover, the text enables readers to master common instrumental methods to perform a broad range of quantitative analyses. Author Brian Tissue has written and structured the text so that readers progressively build their knowledge, beginning with the most fundamental concepts and then continually applying these concepts as they advance to more sophisticated theories and applications. Basics of Analytical Chemistry and Chemical Equilibria is clearly written and easy to follow, with plenty of examples to help readers better understand both concepts and applications. In addition, there are several pedagogical features that enhance the learning experience, including: Emphasis on correct IUPAC terminology "You-Try-It" spreadsheets throughout the text, challenging readers to apply their newfound knowledge and skills Online tutorials to build readers' skills and assist them in working with the text's spreadsheets Links to analytical methods and instrument suppliers Figures illustrating principles of analytical chemistry and chemical equilibria End-of-chapter exercises Basics of Analytical Chemistry and Chemical Equilibria is written for undergraduate students who have completed a basic course in general chemistry. In addition to chemistry students, this text provides an essential foundation in analytical chemistry needed by students and practitioners in biochemistry, environmental science, chemical engineering, materials science, nutrition, agriculture, and the life sciences.
Principles of Analytical Chemistry gives readers a taste of what the field is all about. Using keywords of modern analytical chemistry, it constructs an overview of the discipline, accessible to readers pursuing different scientific and technical studies. In addition to the extremely easy-to-understand presentation, practical exercises, questions, and lessons expound a large number of examples.
Since the last revision of this book in 1999, there has been tremendous development in the field of Analytical Chemistry. In view of this, the book has been thoroughly revised as well as enlarged.Thus, in the field of separation science, 3 new chapters (i) Super critical fluid chromatography and extraction (ii) Electrophoresis (iii) Capillary electrophoresis & Capillary electro-chromatography have been added. The two original chapters on chromatography general and ion exchange separations have been totally redrafted in view of new theories on exchange phenomena.In the field of Chromatography 4 new chapters have been added. They are (i) X-ray spectroscopy (ii) Mossbauer spectroscopy (iii) Raman spectroscopy, and (iv) Electron microscopy.In frontier areas, three new chapters on (i) Chemiluminescence, Atomic fluorescence ionisation spectroscopy (ii) Chemical sensors & Biological sensors (iii) Refractometry & Interferometry have been added.In addition, in twenty chapters new material has been added principally dealing with statistical methods in analytical chemistry, newer supramolecular compounds like rosaxene, use of hyphenatical technique in gas chromotometry & mass spectrometry, spectro-electrochemistry, several kinds of interference in AAS, UV photoelectron spectroscopy, hydrodynamic voltametery, etc.The limited and relevant references are retained to literature of those books which are easily accessable. The overall planning has been done so as not to leave out any upcoming area in analytical chemistry. The book will be indispensable for postgraduate students majoring in analytical chemistry and chemistry graduates in general to keep track of recent developments. It will also serve as guide to the practising chemistry & research investigators to get acquainted in newer areas of chemical sciences.Contents ?Introduction ?Reliability of Analytical Data and Statistical Analysis ?Sampling in Analysis ?Gravimetric Analysis ?Volumetric Analysis?Acid Base Titrations ?Redox Titrations ?Precipitation Titrations Complexometric (EDTA) Titrations ?Solvent Extraction ?Supramolecules in Solvent Extraction ?Principles of Chromatography ?Ion Exchange Chromatography ?Ion Chromatography ?Adsorption Chromatography ?Partition Chromatography ?Gas Chromatography ?High Performance Liquid Chromatography ?Supercritical Fluid Chromatography and Extraction ?Exclusion Chromatography ?Electrochromatography ?Electrophoresis ?Capillary Electrophoresis ?Analytical Spectroscopy ?Ultraviolet and Visible Spectrophotometry ?Infrared Spectroscopy ?Raman Spectroscopy ?Atomic Absorption Spectroscopy ?Atomic Emission Spectroscopy ?Inductively Coupled Plasma?Atomic Emission Spectroscopy ?Chemiluminescence, Atomic Fluorescence and Ionisation Spectroscopy ?Molecular Luminescence Spectroscopy ?Nephelometry and Turbidimetry ?Refractometry and Interferometry ?Polarimetry and Related Methods ?Nuclear Magnetic Resonance Spectroscopy ?Electron Spin Resonance Spectroscopy ?X-Ray Spectroscopy ?Mossbauer Spectroscopy ?Electron Spectroscopy ?Electron Microscopy ?Photoacoustic Spectroscopy ?Mass Spectrometry ?Thermoanalytical Methods ?Radioanalytical Techniques ?Electroanalytical Methods: Potentiometry ?Polarography and Voltammetric Methods ?Conductometric Methods ?Coulometry and Electro Deposition Methods ?Chemical Sensors and Biosensors ?On-line Analysers-Automated Instrumentation Methods ?Answers to the Problems ?Index.
A comprehensive study of analytical chemistry providing the basics of analytical chemistry and introductions to the laboratory Covers the basics of a chemistry lab including lab safety, glassware, and common instrumentation Covers fundamentals of analytical techniques such as wet chemistry, instrumental analyses, spectroscopy, chromatography, FTIR, NMR, XRF, XRD, HPLC, GC-MS, Capillary Electrophoresis, and proteomics Includes ChemTech an interactive program that contains lesson exercises, useful calculators and an interactive periodic table Details Laboratory Information Management System a program used to log in samples, input data, search samples, approve samples, and print reports and certificates of analysis
Analytical Chemistry, Second Edition covers the fundamental principles of analytical chemistry. This edition is organized into 30 chapters that present various analytical chemistry methods. This book begins with a core of six chapters discussing the concepts basic to all of analytical chemistry. The fundamentals, concepts, applications, calculations, instrumentation, and chemical reactions of five major areas of analytical chemistry, namely, neutralization, potentiometry, spectroscopy, chromatography, and electrolysis methods, are emphasized in separate chapters. Other chapters are devoted to a discussion of precipitation and complexes in analytical chemistry. Principles and applications and the relationship of these reactions to the other areas are stressed. The remaining chapters of this edition are devoted to the laboratory. A chapter discusses the basic laboratory operations, with an emphasis on safety. This topic is followed by a series of experiments designed to reinforce the concepts developed in the chapters. This book is designed for introductory courses in analytical chemistry, especially those shorter courses servicing chemistry majors and life and health science majors.
Balances old and new methods of chemical analysis by treating classic topics such as volumetric and gravimetric methods as well as newer areas including solvent extraction and chromatographic methods of separation. Emphasizes fundamental principles of each method and indicates possible applications to other areas of chemistry. It can be used as both a textbook for postgraduate students majoring in analytical chemistry and a reference for practicing analytical chemists and researchers.
The complex field of analytical chemistry requires knowledge and application of the fundamental principles of numerical calculation. Problems of Instrumental Analytical Chemistry provides support and guidance to help students develop these numerical strategies to generate information from experimental results in an efficient and reliable way. Exercises are provided to give standard protocols to follow which address the most common calculations needed in the daily work of a laboratory. Also included are easy to follow diagrams to facilitate understanding and avoid common errors, making it perfect as a hands-on accompaniment to in-class learning. Subjects covered follow a course in analytical chemistry from the initial basics of data analysis, to applications of mass, UV-Vis, infrared and atomic spectrometry, chromatography, and finally concludes with an overview of nuclear magnetic resonance. Intended as a self-training tool for undergraduates in chemistry, analytic chemistry and related subjects, this book is also useful as a reference for scientists looking to brush up on their knowledge of instrumental techniques in laboratories. Request Inspection Copy